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|Title: ||Study on the mechanical and thermal degradation properties of hybrid composites containing rice husk, short glass fibre and polypropylene|
|Other Titles: ||Dao gu fen ji duan bo li xian wei fu he cai liao zhi ji xie ji re xiang jie xing neng yan jiu|
|Authors: ||Yip, Chui Ling (葉翠玲)|
|Department: ||Department of Physics and Materials Science|
|Degree: ||Master of Philosophy|
|Issue Date: ||2008|
|Publisher: ||City University of Hong Kong|
|Subjects: ||Fibrous composites -- Mechanical properties.|
|Notes: ||CityU Call Number: TA418.9.C6 Y57 2008|
xiii, 124 leaves : ill. 30 cm.
Thesis (M.Phil.)--City University of Hong Kong, 2008.
Includes bibliographical references (leaves 113-123)
|Abstract: ||This study aims to investigate the mechanical and thermal properties of hybrid
composites containing rice husk (RH), glass fibres (GF) and polypropylene (PP). The
objective is to develop the required technology for industrial applications of natural fibres
In this study, both binary RH/PP composites and ternary RH/GF/PP hybrid
composites had been prepared for investigation. As RH fillers are commercially available
in two different forms: rice husk flake (RF) and rice husk powder (RP), their reinforcing
effect were also investigated. In order to enhance the interfacial bonding of glass fibre or
rice husk with the polypropylene matrix, maleic anhydride grafted polypropylene (MA-g-
PP) was used as the compatibilizing agent.
In this work, a series of measurements of mechanical, thermal, and water
absorption behaviour were conducted to investigate the performance of the obtained
composites. The stiffness and fracture resistance of composites were measured by using
tensile, flexural, Izod impact, instrumental drop weight impact and the essential work of
fracture analysis. Following the mechanical tests, fractography, glass fibres length
distribution and orientation were investigated by using scanning electron microscope
(SEM), optical microscope and image analysis software. Besides, the water absorption
curves and the influences of moisture content to the stiffness of composites were also
determined. Finally, the thermal and processing properties of the composites were
characterized by using thermogravimetry analysis and rheology measurement.
It was found that the application of rice husks and glass fibres brought positive
effects to the performance of composites. The addition of RH fillers and glass fibres
effectively enhanced the stiffness of composites. However, the content and size of RH or
GF affected the interfacial adhesion, orientation and dispersion of them. Up to 20wt% of
GF were introduced, the reinforcement effect was reduced.
The water absorption behaviour and the influences of water immersion content
towards the mechanical strength of composites were illustrated. It was found that the time
for achieving saturation and the absorbed moisture content at the equilibrium state was
directly proportional to the rice husk content. The bending strength of the composites
dropped gradually within the water immersion period.
In the thermogravimetric studies, the changes of mass of binary and ternary
composites were monitored under different heating rates. And the influences of RF and GF
on thermal decomposition behaviours of PP matrix were illustrated. The faster the heating
rate, the higher the degradation temperature was obtained. Besides, RF was thermally stable.
The result showed that the addition of RF could retard the thermal decomposition of PP in
the composites. The RH turned to carbon char after degradation to protect and enhance the
thermal stability of PP matrix. However, the presence of RF in the composites did not
affect the degradation mechanism of PP.|
|Online Catalog Link: ||http://lib.cityu.edu.hk/record=b2340580|
|Appears in Collections:||AP - Master of Philosophy |
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